2.3 A glimpse at the spectrometer在线视频

Nuclear Magnetic Resonance Spectroscopy in Organic Chemistry课程列表：

Chapter 1 Introduction

-1. Introduction

Chapter 2 Basic Concepts

-2.1 Properties of nuclei and the phenomenon of nuclear magnetic resonance

-2.2 Precession of nuclei and the detection of signals

-2.3 A glimpse at the spectrometer

-Homework

Chapter 3 1H NMR

-3.1.1 Definition of chemical shift

-3.1.2.1 Influencing factors on chemical shifts --- inductive effect

-3.1.2.2 Influencing factors on chemical shifts --- anisotropic

-3.1.2.3 Influencing factors on chemical shifts --- resonance

-3.1.3 Chemical shifts of proton

-3.2.1.1 N+1 rule and splitting patterns --- equivalent splitting

-3.2.1.2 Splitting patterns --- nonequivalent splitting

-3.2.2.1 Magnitude of coupling constants and Karplus rule

-3.2.2.2 Magnitude of coupling constants and Karplus rule --- examples

-3.2.3.1 First order spin systems

-3.2.3.2 Second order AB systems

-3.3 Coupling from heteronuclei

-3.4 Protons on heteroatoms

-Homework

Chapter 4 13C NMR

-4.1 Decoupled 13C spectra

-4.2 Chemical shifts of 13C

-4.3 Edited 13C spectra

-Homework

Chapter 5 Multinuclear NMR

-5. Multinuclear NMR other than 13C

-Homework

Chapter 6 Introduction to multi-dimensional NMR techniques

-6. Introduction to multi-dimensional NMR techniques

Chapter 7 Homonuclear two-dimensional NMR

-7.1 Homonuclear two-dimensional NMR --- COSY

-7.2 Homonuclear two-dimensional NMR --- NOESY

-7.3 Case study --- COSY & NOESY

Chapter 8 Heteronuclear two-dimensional NMR

-8.1 Heteronuclear two-dimensional NMR --- HMQC HSQC

-8.2 Heteronuclear two-dimensional NMR --- HMBC

-Homework

Chapter 9 Experimental considerations

-9.1 Experimental considerations --- sample preparation

-9.2 Experimental considerations --- parameter setting

-Homework

Chapter 10 Review

-10 Review

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